用於太陽能電池應用的茚並異喹啉類有機化合物的設計與合成

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蘇柏都(Suri Babu Akula) 查詢紙本館藏

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論文名稱

用於太陽能電池應用的茚並異喹啉類有機化合物的設計與合成
(Design and Synthesis of Indenoisoquinoline-Based Organic Compounds for Solar Cell Applications)

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摘要(中)

目前新型有機染料敏化太陽能電池專注於化合物的設計，合成和性質。茚諾喹啉（IQN）化合物是一種拓撲異構酶I抑製劑，最有活性的抗癌劑之一，並且具有良好的化學穩定性和可見光吸收寬廣的特性，其在於IQN核心是相連共軛四環系統，所以適合應用於染料敏化太陽能電池。
此論文之設計原理和策略，在於利用IQN作為開發新的有機化合物之核心，並合成多種基於茚並異喹啉的新化合物，分別利用於染料敏化太陽能電池的染料和鈣鈦礦太陽能電池中的電洞傳輸層。這些合成出來的化合物，光學和電子性質是適合用於此兩種領域，而且除了以上性質之外，也同時在持續探討其他光電特性

摘要(英)

The current studies were focused on the design, synthesis, and characterization of new organic compounds for applications in solar cells. Indenoisoquinoline (IQN) compounds are a class of topoisomerase I inhibitors, one of the most active anti-cancer agents and have high chemical stability as well as broad absorption characteristics in the visible region. The IQN core is a tetracyclic fused conjugated system of indene and isoquinoline, which provides an extended conjugation. In the following, the design principle and strategies to utilize the IQN core as a building block in the development of new organic compounds will be discussed. Various new compounds based on indenoisoquinoline were synthesized to be employed as sensitizers and hole transporting layers in dye sensitized solar cells and perovskite solar cells, respectively. The optical and electronic properties of these compounds are apparently promising and their photovoltaic properties are under investigation.

關鍵字(中)

★ 染料敏化太陽能電池
★ 茚並異喹啉類染料
★ 鈣鈦礦太陽能電池
★ 空孔運輸材料
★ 基於茚基異喹啉的HTMs

關鍵字(英)

★ Dye sensitized solar cells
★ Indenoisoquinoline-based dyes
★ Perovskite solar cells
★ Hole transport materilas
★ Indenoisoquinoline based HTMs

論文目次

Table of Contents
Abstract i
Acknowledgements ii

Chapter 1
1 Introduction to the Solar Cell 1
1.1 Dye sensitized solar cells 2
1.2 Components of the dye sensitized solar cells 3
1.2.1 Nanocrystalline semiconductor oxide film electrode 3
1.2.2 Light absorbers 5
1.2.2.1 Inorganic dyes based on ruthenium for DSSC applications: 6
1.2.2.2 Metal free organic dyes for DSSC applications: 8
1.2.3 Electrolytes 10
1.2.3.1 Liquid electrolytes 10
1.2.3.2 Solid electrolytes 11
1.2.3.3 Quasi-solid electrolyte 12
1.2.4 Counter electrodes 12
1.2.5 Transparent conducting substrate (TCO) 13
1.3 Assembling of dye sensitizer solar cell34 13
1.4 Mechanism 14
1.4.1 Operating Principles68 14
1.4.2 Limitations 15
1.5 Efficiency of solar cell 16
1.6 Perovskite solar cells 18
1.6.1 Organometallic halide perovskite based solar cells 19
1.6.1.1 Light absorbers: 19
1.6.1.2 Hole transport materials (HTMs): 21
1.6.1.3 Working Principle and limitation: 24
1.7 Motivation of Research 26
Chapter 2
Synthesis and Characterization of Indenoisoquinoline-Based Dye Sensitizers for Dye-Sensitized Solar Cell Applications 28
2.1 Introduction 28
2.2 Synthesis 30
2.3 Results 34
2.3.1 Optical Properties of IQ dyes 34
2.3.2 Electronic Properties: 35
2.3.4 Efficiency of DSSCs based on IQ dyes: 37
Chapter 3
Synthesis and Characterization of Indenoisoquinoline-Based Hole Transporting Layers for Application in Perovskite Solar Cells 38
3.1 Introduction 38
3.2 Synthesis 40
3.3 Results 43
3.3.1 Optical properties: 43
3.3.2 Electronic properties: 44
3.4 Performances of Perovskite cells based on DIQ dyes: 46
Chapter 4
4 Experimental Section 47
4.1 Physicochemical Methods 47
4.2 Preparation of TiO2 Electrodes and DSSC Device 47
4.3 DSSC Performance Measurements 49
4.4 Experimental procedures for syntheses of IQN based sensitizers 50
4.5 Experimental procedures for syntheses of IQN based HTMs 64
References 71

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指導教授

李文仁(Wen-Ren Li)

審核日期

2017-7-28

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