超音波噴塗結合真空萃取技術於大氣環境下製備全無機CsPbI2Br鈣鈦礦太陽能電池

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游育典(Yu-Tien Yu) 查詢紙本館藏

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化學工程與材料工程學系

論文名稱

超音波噴塗結合真空萃取技術於大氣環境下製備全無機CsPbI2Br鈣鈦礦太陽能電池
(Ultrasonic Spray-Assisted Method via Vacuum-Extraction Technique for All-inorganic CsPbI2Br Perovskite Solar Cells under Ambient Condition.)

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★ 利用超音波噴塗技術製備鈣鈦礦薄膜於太陽能電池元件之應用	★ 利用溶液剪切力塗佈法製作高效能DTTRQ小分子 N 型有機場效電晶體元件
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★ 利用兩步驟超音波噴塗技術製備平面型p-i-n結構鈣鈦礦太陽能電池元件之應用	★ 透明氧化物薄膜電晶體與電晶體式記憶體之分析與應用
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★ 剪切力溶液製程應用於高效能有機薄膜電晶體：含硒碳鏈聯?吩小分子半導體材料	★ 利用超音波噴塗技術製備混合有機陽離子鈣鈦礦太陽能電池

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摘要(中)

近年來，有機無機混成鈣鈦礦太陽能電池效率急劇發展，至今年為止效率已有顯著地突破，其轉換效率已可媲美市面上主流多晶矽太陽能電池，由於其可藉由調變鈣鈦礦組成元素成分，進而調整半導體能隙大小以及表面形貌，且可以溶液製程製備太陽能電池，大幅降低製程上的成本，故作為太陽能電池裝置，鈣鈦礦是未來極具潛力的材料。但目前有機無機混成鈣鈦礦太陽能電池熱穩定性不佳，且尚缺乏可放大太陽能電池面積與連續生產之有效製程方法。
是故，本實驗透過調變鈣鈦礦結構，並使用超音波噴塗法結合真空萃取技術，在大氣環境下成功製備全無機鈣鈦礦CsPbI2Br太陽能電池。利用無機元素銫(Cs+)取代有機陽離子甲胺(MA+)、甲脒(FA+)，解決有機陽離子受高溫會逸散的問題，藉此提升鈣鈦礦太陽能電池的熱穩定性。此外，製程上使用超音波噴塗設備，提供了大面積與連續製程的可能性，對於太陽能電池工業化生產做出了良好的示範。再者，結合真空萃取技術(Vacuum-Extraction Technique)，有效解決結晶成核過程與退火長晶過程的競爭關係，以形成平整且光滑的高品質鈣鈦礦薄膜，在製程優化後，再由添加醋酸鉛(Pb(Ac)2)改變鈣鈦礦成膜性質，獲得最高光電轉換效率10.06%，由太陽能電池特性曲線獲得開路電壓1.12 V、短路電流密度13.99 mA cm-2及填充因子64.81%，提供了另一種形式在大氣下製備穩定的全無機鈣鈦礦太陽能電池。

摘要(英)

All-inorganic cesium-based CsPbX3 perovskite solar cells are regarded as one of most promising forms due to the superior thermal stability compared to organic-inorganic hybrid perovskite. However, it has been challenging to achieve these high-quality films over large areas using scalable methods under realistic ambient conditions. Herein, we investigate the perovskite crystal growth and morphology control by vacuum-assisted strategy for ambient scalable ultrasonic spray coating fabrication of all-inorganic CsPbI2Br perovskite films. As a result, the process can produce highly crystalline, uniform, and pinhole-free CsPbI2Br films and the planar structure of perovskite solar cells based on ITO/SnO2/CsPbI2Br/PTAA/Au were fabricated. Moreover, additive engineering strategies of Lead(II) acetate (Pb(Ac)2) were used to address the defect of perovskite nanocrystal. Ultimately, the optimized CsPbI2Br perovskite solar cells shows maximum power conversion efficiency (PCE) of 10.06% with a open-circuit voltage (Voc) of 1.12 V, short-circuit current density (Jsc) of 13.99 mA cm-2, and fill factor (FF) of 64.81%. Overall, we demonstrated the high throughput ultrasonic spray-coating method as a lab‐to‐fab translation tool for solution‐processed of all-inorganic CsPbI2Br perovskite films at ambient condition.

關鍵字(中)

★ 鈣鈦礦
★ 全無機鈣鈦礦
★ 鈣鈦礦太陽能電池
★ 真空萃取
★ 超音波噴塗

關鍵字(英)

★ Perovskite
★ All-inorganic perovskite
★ Perovskite solar cells
★ Vacuum-extraction
★ Ultrasonic spray-coating

論文目次

摘要 i
Abstract ii
謝誌 iii
目錄 iv
圖目錄 vi
表目錄 ix
第一章緒論 1
1-1 前言 1
1-2 太陽能電池材料及發展 1
1-3 太陽能電池工作原理及特性 7
1-3-1 工作原理 7
1-3-2 輸出特性 (Output Characteristics) 8
第二章文獻回顧 11
2-1 鈣鈦礦太陽能電池簡介 11
2-1-1 鈣鈦礦發展沿革 11
2-1-2 鈣鈦礦材料結構及特性 12
2-1-3 結構穩定性 14
2-1-4 鈣鈦礦元件結構 17
2-2 鈣鈦礦薄膜製備方法 18
2-2-1 一步驟沉積法 18
2-2-2 兩步驟沉積法 20
2-2-3 雙源共蒸鍍沉積法 21
2-2-4 大面積製程方法 22
2-3 全無機銫鉛鹵鈣鈦礦太陽能電池 32
2-3-1 CsPbI3鈣鈦礦太陽能電池 32
2-3-2 CsPbBr3鈣鈦礦太陽能電池 35
2-3-3 CsPbI2Br鈣鈦礦太陽能電池 38
2-4 研究動機 42
第三章實驗與研究方法 43
3-1 實驗藥品與溶劑 43
3-1-1 實驗儀器 44
3-1-2 元件製作儀器 44
3-1-3 元件測量儀器 45
3-1-4 超音波噴塗霧化設備 47
3-2 實驗步驟及方法 48
3-2-1 鈣鈦礦前驅溶液配置 48
3-2-2 全無機鈣鈦礦太陽能電池元件製作 49
3-3 鈣鈦礦太陽能電池量測 55
第四章結果與討論 56
4-1 真空萃取之影響 56
4-2 醋酸鉛添加濃度之影響 62
第五章結論 70
第六章參考資料 72

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指導教授

劉振良(Cheng-Liang Liu)

審核日期

2020-7-22

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