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    Please use this identifier to cite or link to this item: http://ir.lib.ncu.edu.tw/handle/987654321/28273


    Title: Determination of Fluorescent Whitening Agents in Infant Clothes and Paper Materials by Ion-pair Chromatography and Fluorescence Detection
    Authors: Shu,WC;Ding,WH
    Contributors: 中央大學
    Keywords: PERFORMANCE LIQUID-CHROMATOGRAPHY;SOLID-PHASE EXTRACTION;OPTICAL BRIGHTENERS;LAUNDRY DETERGENTS;MASS-SPECTROMETRY;SURFACE WATERS;SEPARATION
    Date: 2009
    Issue Date: 2010-06-29 19:45:16 (UTC+8)
    Publisher: 化學研究所
    Abstract: A simple and rapid method was developed to simultaneously determine four stilbene-type disulfonate and one distyrylbiphenyl-type fluorescent whitening agents (FWAs) in infant clothes and paper materials by ion-pair chromatography. FWAs were extracted from cloth and papers samples using a hot-water extraction. The aqueous extract was then mixed with ion-pair reagent, extracted with C-18-SPE cartridges and eluted with methanol. The contents of FWAs were determined by an isocratic ion-pair chromatography with RP-C-18 column and equipped with fluorescence detection. Limits of quantitation were 0.04 to 0.45 ng/g in 10 g of samples. Recovery of FWAs in spiked infant cloth and paper samples was between 76 to 92% and precision (RSD) ranging from 2.0 to 4.0%. Analysis of three infant clothes and six paper materials found concentrations of selected FWAs ranging between n.d. to 24 mu g/g and n.d. to 3.8 mu g/g, respectively.
    Relation: JOURNAL OF THE CHINESE CHEMICAL SOCIETY
    Appears in Collections:[化學研究所] 期刊論文

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