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姓名	陳智堯(Chih Yao Chen)  查詢紙本館藏	畢業系所	材料科學與工程研究所
論文名稱	利用表面陽極處理調變液態鎵奈米顆粒形貌及其光學性質 (Oxidation-mediated changes in morphology and optical properties of liquid gallium nanoparticles)
相關論文	★ 開發鎵奈米粒子沉浸於可拉伸聚合物之可調式電漿子結構 ★ 利用等效差分時域(FDTD)模擬分析自組裝鎵奈米顆粒嵌入可拉伸彈性材料光學性質探討 ★ 無鉛銲料錫銀銦與銅基板的界面反應 ★ 高度反射性銀/鑭雙層p型氮化鎵歐姆接觸之性質研究 ★ 以電子迴旋共振化學氣相沉積氫化非晶矽薄膜之熱處理結晶化研究 ★ 研究奈晶矽與非晶矽之多層結構經熱退火處理後之性質及其在PIN太陽能電池吸收層中之應用 ★ 利用陽極氧化鋁模板製備銀奈米結構陣列於玻璃基板 ★ 利用電子迴旋共振化學氣相沉積法沉積氫化非晶矽薄膜探討其應力與結晶行為 ★ 高反射低電阻銀鑭合金P型氮化鎵歐姆接觸之研究 ★ 陽極氧化鋁模板製備銀奈米粒子陣列及其表面增強拉曼散射效應之應用 ★ 製備磷摻雜奈米矽晶氧化矽薄膜及其於太陽能電池之應用 ★ 陽極氧化鋁模板製備銀奈米粒子陣列及其光學性質 ★ 以電流控制方式快速製備孔洞間距400至500奈米之陽極氧化鋁模板 ★ 利用濕式氧化法製備氧化矽薄膜應用於矽晶太陽能電池表面鈍化技術之研究 ★ 磷摻雜矽奈米晶粒嵌入於氮化矽基材之材料成長與特性分析 ★ 利用電子迴旋共振化學氣相沉積法製備多層SiOxNy:H/SiCxNy:H抗反射薄膜及其於矽基太陽能電池之應用
檔案	[Endnote RIS 格式]    [Bibtex 格式]    [相關文章]   [文章引用]   [完整記錄]   [館藏目錄]   至系統瀏覽論文 (2027-4-13以後開放)
摘要(中)	由於鎵金屬本身性質具有無毒、室溫為液態與緻密氧化層等特性，且鎵奈米顆粒有較高的等離子體能量 (plasma energy（14 eV）)，並可藉由改變它們的形狀和大小，來調變局部表面電漿子共振 (localized surface plasmon resonance, LSPR) 特徵範圍，可獲得從紫外波段到可見波段調控的優勢，因此為近年來電漿子學中熱門研究主題之一。 我們利用表面陽極處理方式改變液態鎵奈米顆粒表面形貌而形成窩坑結構(dimple structure)，其中電壓與反應時間將影響鎵奈米顆粒表面凹陷程度，其形成原因來液態鎵金屬表面能變化與氧化層生成時所產生的壓應力造成淺層凹痕，此凹痕導致後續的陽極反應集中於特定區域造成嚴重變形形成dimple結構。透過XPS計算陽極處理過程中氧化層生成之厚度，並利用熱氧化法與FDTD模擬結果說明本研究中氧化層對紅移現象影響有限，藉此證明液態Ga NPs的形貌變化為造成LSPR特徵波峰波長發生紅移現象的主要原因。 利用此方式可調變Ga NPs的LSPR特徵波峰波長之最大紅移量達77 nm左右，透過FDTD模擬不同凹陷程度之光學變化，此結果與實驗結果具有相同趨勢進行，並由近場分佈顯示金屬表面尖端與銳利邊緣區域產生”熱點”(hotspots)，此尖端與銳利邊緣是伴隨凹陷結構所產生。透過此方式我們以短時間(反應時間10秒以內)與簡易製程方式即可調整液態Ga NPs之LSPR特徵波峰波長位置。
摘要(英)	Gallium, whose melting point is near the room temperature, is relatively non-toxic and will form the compact oxide layer. With a bulk plasmon resonance energy of 13.9 eV, Ga has recently been proved to be a good candidate for UV plasmonics with a Drude-like dielectric function extending from the vacuum ultraviolet into the infrared spectral region. In this work, the dimple textures were formed on the surface of gallium nanoparticles (Ga NPs) through the anodization treatment, using the applied voltage and the reaction time to control the degree of deformation. During the treatment, the increasing oxide layer would produce the compression stress, leading the formation of dimple textures. The nanoscale dimple-like textures led to changes in the localized surface plasmon resonance (LSPR) wavelength. A maximal LSPR red-shift of ~77 nm was preliminarily achieved using an anodization voltage of 0.7 V. The finite-difference time-domain (FDTD) simulations also suggested that the LSPR tunability was primarily determined by the shape of the deformed particles, which was also in good agreement with the trend in the LSPR shift obtained from the experimental results. The near electric field simulated by FDTD was concentrated near spikes or narrow walls, and thus the hotspots could clearly be observed. The extent of particle deformation could be adjusted in a very short period of anodization time (~7 s), which offers an efficient way to tune the LSPR response of Ga NPs.
關鍵字(中)	★ 陽極處理 ★ 局域性表面電漿子共振 ★ 液態鎵奈米顆粒	關鍵字(英)	★ Anodization ★ Localized surface plasmon resonance ★ liquid gallium nanoparticles
論文目次	摘要 i Abstract ii 致謝 iii 第一章 緒論 1 第二章 文獻回顧 2 2-1電漿子光學 (Plasmonic) 2 2-1-1電漿子光學的發展 2 2-1-2表面電漿子共振 2 2-1-3影響電漿子共振的因素 3 2-2鎵 9 2-2-1鎵奈粒子之LSPR特徵 10 2-2-2氧化鎵層對電漿子共振的影響 11 2-2-3外加電壓對液態鎵金屬形貌變化之影響 13 2-3電漿子光學調控方法 14 2-3-1調變液體溶液的pH值 14 2-3-2電化學氧化還原反應 15 2-3-3機械式變形可撓式彈性體基板 16 第三章 研究方法 17 3-1研究動機與實驗架構 17 3-2 實驗步驟 18 3-3製程設備與分析儀器 18 3-4有限差分時域法(FDTD)模擬液態鎵奈米顆粒之設置架構 19 第四章 結果與討論 21 4-1陽極處理液態鎵奈米顆粒之探討 21 4-1-1 探討不同厚度下鎵奈米顆粒分佈特性 21 4-1-2探討陽極處理對鎵奈米顆粒形貌變化之影響 22 4-1-3 探討陽極處理過程中氧化層對Ga NPs形貌變化之影響 28 4-1-4 探討不同反應電壓下對鎵奈米顆粒之影響 32 4-2表面陽極處理之液態Ga NPs光學性質 35 4-2-1 探討影響Ga NPs的LSPR特徵波長之因素 35 4-2-2模擬陽極處理Ga NPs之LSPR特性 39 第五章結論 43 參考文獻 44
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指導教授	陳一塵(I Chen Chen)	審核日期	2022-4-14
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