博碩士論文 92324039 完整後設資料紀錄

DC 欄位 語言
DC.contributor化學工程與材料工程學系zh_TW
DC.creator徐啟鐘zh_TW
DC.creatorChi-Chung Hsuen_US
dc.date.accessioned2005-7-20T07:39:07Z
dc.date.available2005-7-20T07:39:07Z
dc.date.issued2005
dc.identifier.urihttp://ir.lib.ncu.edu.tw:444/thesis/view_etd.asp?URN=92324039
dc.contributor.department化學工程與材料工程學系zh_TW
DC.description國立中央大學zh_TW
DC.descriptionNational Central Universityen_US
dc.description.abstract本研究以間苯二甲酸及5-硝基間苯二甲酸為原料,製備双-1,3,4-zh_TW
dc.description.abstractThis research is with isophthalic acid and 5-nitroisophthalic acid, as raw materials. Prepare bis-1,3,4-oxadiazole series chemical compounds. Can all win the purpose thing in accordance with the method step of papers. Among them every bis-1,3,4-oxadiazole series chemical compounds all shows the absorption peak of 1724 cm-1 on IR spectrum. Unknown it where characteristic of part absorb and how analyze for chemical compound. Every bis-1,3,4-oxadiazole series chemical compounds have nitro group all simple antithetical couplet when NH2NH2/Pd-C method is reduced for the amine group. This kind of amine group can also condensation reaction with the Cyanuric chloride. And become the water soluble chemical compounds. 5-nitroisophthalic acid can have azobenzene while reducing in the zinc powder-NaOH’’s aqueous solution, and the rate is 90%. This azobenzene has four formic acid. Can all esterify, Hydrazine hydrate and benzoyl chloride. Cyclodehydration is used in phosphorus oxychloride to be azobenzene with four pieces of 1,3,4-oxadiazole. The above-mentioned chemical compounds formate the purpose and increase its fluorescence intensity or the fluorescence of different wavelength emerges because of increase of 1,3,4-oxadiazole in the income result. Cause because of azobenzene(-N=N-) of the result. Fail to increase its fluorescence intensity and wavelength.en_US
DC.subject5-硝基間苯二甲酸zh_TW
DC.subject間苯二甲酸zh_TW
DC.subject5-nitroisophthalic aciden_US
DC.subjectisophthalic aciden_US
DC.subjectoxadiazoleen_US
DC.title合成1,3-双[5-苯基-1,3,4-zh_TW
dc.language.isozh-TWzh-TW
DC.type博碩士論文zh_TW
DC.typethesisen_US
DC.publisherNational Central Universityen_US

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